6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

Base Information

Chemical Name:6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine
CAS No.:1242460-59-8
Molecular Formula:C₅₀H₅₇N₅O₉S
Molecular Weight:904.097
Hs Code.:

Synonyms:6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

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Chemical Property of 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

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Technology Process of 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

There total 1 articles about 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1225490-82-3
6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1242460-59-8
6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

Guidance literature:: With pyridine; at 20 ℃; for 1h; regioselective reaction;
DOI:10.1080/15257770903155576

Reference yield: 77.0%

: 1242460-59-8
6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1225490-83-4
6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine-3'-O-(2-cyanoethyl)(N,N-diisopropyl)phosphoramidite

Guidance literature:: 6-S-{2-[(2-ethylhexyl)oxycarbonyl]ethyl}-5'-O-(4,4'-dimethoxytrityl)-2-N-phenoxyacetyl-2'-deoxy-6-thioguanosine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.416667h;

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1080/15257770903155576