Technology Process of 4-(3,3-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl)benzaldehyde
There total 6 articles about 4-(3,3-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl)benzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 0 - 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol403338s
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 25 °C / Schlenk technique; Inert atmosphere; Cooling with ice
2: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
With
diisobutylaluminium hydride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; toluene;
2: |Dess-Martin Oxidation;
DOI:10.1021/ol403338s
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / toluene; mineral oil / 1 h / 20 °C / Inert atmosphere; Schlenk technique
1.2: 12 h / 110 °C / Inert atmosphere; Schlenk technique; Sealed tube
2.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / 25 °C / Schlenk technique; Inert atmosphere; Cooling with ice
3.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
With
sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
3.1: |Dess-Martin Oxidation;
DOI:10.1021/ol403338s
