(((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane

Base Information

• Chemical Name: (((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane
• CAS No.: 930121-22-5
• Molecular Formula: C₁₆H₁₆N₂O
• Molecular Weight: 252.316
• Mol file: 930121-22-5.mol

Synonyms:(((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane

Chemical Property of (((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane

There total 1 articles about (((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

pyrrole (109-97-7,30604-81-0) + 4-Hydroxyacetophenone (99-93-4) → (((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane (930121-22-5)

Guidance literature:

With L-Tartaric acid; N,N'-Dimethylurea; In neat (no solvent); at 70 ℃; Green chemistry;

DOI:10.1039/d1gc01515j

Reference yield: 85.0%

(((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane (930121-22-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → C18H16N2O3

Guidance literature:

(((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane; N,N-dimethyl-formamide; With trichlorophosphate; at 80 ℃; for 6h;

With sodium carbonate; In water; at 80 ℃; for 2h;

DOI:10.1080/10610278.2017.1372581

Reference yield: 78.0%

(((p-hydroxyphenyl)methyl)bispyrrol-2-yl)methane (930121-22-5) + penta(ethylene glycol) bis(p-toluenesulfonate) (41024-91-3) → C42H50N4O6 (1379801-51-0)

Guidance literature:

With potassium carbonate; In acetonitrile; for 12h; Reflux;

DOI:10.1002/chem.201103239

upstream raw materials:

pyrrole

4-Hydroxyacetophenone

Downstream raw materials:

C₄₂H₅₀N₄O₆