9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole

Base Information

• Chemical Name: 9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole
• CAS No.: 1357174-22-1
• Molecular Formula: C₄₁H₃₅N₅
• Molecular Weight: 597.762
• Mol file: 1357174-22-1.mol

Synonyms:9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole

Chemical Property of 9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole

There total 1 articles about 9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,3'-[(9-benzyl-9H-carbazole-3,6-diyl)bis(4,1-phenylene)]bis(4-hydroxypent-3-en-2-one) (1357174-26-5) → 9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole (1357174-22-1)

Guidance literature:

With hydrazine hydrate; In ethanol; for 12h; Reflux;

DOI:10.1021/ic202407b

Reference yield: 55.0%

9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole (1357174-22-1) + [(4,4′-dimethylbipyridine)2Pd2(NO3)2](NO3)2 → [(4,4'-dimethyl-2,2'-bipyridine)4Pd4(9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole)2](NO3)4

Guidance literature:

In water; acetone; stirring at room temp. for 2 h, then heated (60°C, 24 h); elem. anal.;

DOI:10.1021/ic202407b

Reference yield:

9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole (1357174-22-1) → [(4,4'-dimethyl-2,2'-bipyridine)4Pd4(9-benzyl-3,6-bis[4-(3,5-dimethyl-1H-pyrazol-4-yl)phenyl]-9H-carbazole)2](BF4)4*3H2O

Guidance literature:

Multi-step reaction with 2 steps

1: water; acetone

2: methanol

In methanol; water; acetone;

DOI:10.1021/ic202407b

upstream raw materials:

3,3'-[(9-benzyl-9H-carbazole-3,6-diyl)bis(4,1-phenylene)]bis(4-hydroxypent-3-en-2-one)