C₄₄H₆₀O₉Si

Base Information

Chemical Name:C₄₄H₆₀O₉Si
CAS No.:872525-92-3
Molecular Formula:C₄₄H₆₀O₉Si
Molecular Weight:761.04
Hs Code.:

C<sub>44</sub>H<sub>60</sub>O<sub>9</sub>Si

Synonyms:C₄₄H₆₀O₉Si

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Chemical Property of C₄₄H₆₀O₉Si

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Technology Process of C₄₄H₆₀O₉Si

There total 19 articles about C₄₄H₆₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 872525-91-2
C₄₄H₆₀O₉Si

: 872525-92-3
C₄₄H₆₀O₉Si

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; for 0.333333h; Heating;
DOI:10.1139/v05-042

Reference yield: 32.0%

: 872525-95-6
C₄₄H₅₈O₉Si

: C₄₁H₅₄O₈Si

: 872525-92-3
C₄₄H₆₀O₉Si

Guidance literature:: With acetic acid; zinc; In ethanol; at 80 ℃; for 4h;
DOI:10.1139/v05-042

Reference yield:

: 872525-98-9
(3aR,7aS)-2,2-Dimethyl-6-oxo-3a,6,7,7a-tetrahydro-benzo[1,3]dioxole-5-carbaldehyde

: 872525-92-3
C₄₄H₆₀O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1: 77 percent / cesium carbonate / CH₂Cl₂ / 2 h / 20 °C

2: 86 percent / morpholine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran / 0.08 h / 20 °C

3: 99 percent / LiAlH[OC(C₂H₅)3]3 / tetrahydrofuran / 1 h / 0 °C

4: 71 percent / diisopropylethylamine / CH₂Cl₂ / 16 h / 20 °C

5: 28 percent / potassium hexamethyldisilazide / tetrahydrofuran; toluene / 0.5 h / Heating

6: 96 percent / Ne₄NHB(OAc)3; acetic acid / acetonitrile / 19 h / -20 - 0 °C

7: 93 percent / camphorsulfonic acid / acetone / 1 h / 20 °C

8: 86 percent / potassium hexamethyldisilazide / tetrahydrofuran; toluene / 0.33 h / Heating

With morpholine; lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride; Ne₄NHB(OAc)3; camphor-10-sulfonic acid; potassium hexamethylsilazane; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; acetone; toluene; acetonitrile; 5: aldol condensation / 8: aldol condensation;
DOI:10.1139/v05-042