7-hydroxyindan-1-one (S,S)-stilbenediol acetal

Base Information

Chemical Name:7-hydroxyindan-1-one (S,S)-stilbenediol acetal
CAS No.:864058-53-7
Molecular Formula:C₂₃H₂₀O₃
Molecular Weight:344.41
Hs Code.:

Synonyms:7-hydroxyindan-1-one (S,S)-stilbenediol acetal

Suppliers and Price of 7-hydroxyindan-1-one (S,S)-stilbenediol acetal

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Chemical Property of 7-hydroxyindan-1-one (S,S)-stilbenediol acetal

Chemical Property:

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Technology Process of 7-hydroxyindan-1-one (S,S)-stilbenediol acetal

There total 4 articles about 7-hydroxyindan-1-one (S,S)-stilbenediol acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864058-55-9
7-acryloyloxyindan-1-one (S,S)-stilbenediol acetal

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 864058-53-7
7-hydroxyindan-1-one (S,S)-stilbenediol acetal

: 934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7,120-74-1
5-norbornene-endo-2-carboxylic acid

Guidance literature:: 7-acryloyloxyindan-1-one (S,S)-stilbenediol acetal; cyclopenta-1,3-diene; With diethylaluminium chloride; In hexane; toluene; at -78 ℃; for 0.166667h;

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 40h;
DOI:10.1139/v05-052

Reference yield:

: 6968-35-0
7-hydroxy-indan-1-one

: 864058-53-7
7-hydroxyindan-1-one (S,S)-stilbenediol acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / pyridine / CH₂Cl₂ / 19 h / 0 - 20 °C

2: 83 percent / para-toluenesulfonic acid monohydrate / benzene / 40 h / Heating

3: 90 percent / LiOH / tetrahydrofuran; H₂O / 40 h / 20 °C

With pyridine; lithium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water; benzene;
DOI:10.1139/v05-052

Reference yield:

: 2325-10-2
(S,S)-hydrobenzoin

: 864058-53-7
7-hydroxyindan-1-one (S,S)-stilbenediol acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / para-toluenesulfonic acid monohydrate / benzene / 40 h / Heating

2: 90 percent / LiOH / tetrahydrofuran; H₂O / 40 h / 20 °C

With lithium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; water; benzene;
DOI:10.1139/v05-052