2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

Base Information

Chemical Name:2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid
CAS No.:133473-10-6
Molecular Formula:C₃₁H₃₃NO₆
Molecular Weight:515.606
Hs Code.:

Synonyms:2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

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Chemical Property of 2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

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Technology Process of 2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

There total 4 articles about 2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133473-09-3
methyl 2-[(9-phenylfluoren-9-yl)amino]-2-deoxy-3,4:5,6-di-O-isopropylidene-D-mannonate

: 133473-10-6
2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

Guidance literature:: With lithium hydroxide; In 1,4-dioxane; water; at 60 ℃; for 20h; Yield given;
DOI:10.1021/jo00011a047

Reference yield:

: 117462-55-2
methyl 2-azido-2-deoxy-3,4:5,6-di-O-isopropylidene-D-mannonate

: 133473-10-6
2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / ethyl acetate / 24 h / 760 Torr

2: Pb(NO₃)2, Et₃N / CH₂Cl₂ / 48 h / Ambient temperature

3: LiOH*H₂O / dioxane; H₂O / 20 h / 60 °C

With lithium hydroxide; lead(II) nitrate; hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; water; ethyl acetate;
DOI:10.1021/jo00011a047

Reference yield:

: 55135-66-5
9-bromo-9-phenyl-9H-fluorene

: 133473-10-6
2-<(9-phenylfluoren-9-yl)amino>-2-deoxy-3,4:5,6-di-O-isopropylidenemannosaminic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Pb(NO₃)2, Et₃N / CH₂Cl₂ / 48 h / Ambient temperature

2: LiOH*H₂O / dioxane; H₂O / 20 h / 60 °C

With lithium hydroxide; lead(II) nitrate; triethylamine; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo00011a047