N₆-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N₆-methyladenosine

Base Information

• Chemical Name: N₆-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N₆-methyladenosine
• CAS No.: 1184837-80-6
• Molecular Formula: C₃₀H₄₂ClN₅O₅Si
• Molecular Weight: 616.232

Synonyms:N₆-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N₆-methyladenosine

Chemical Property of N₆-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N₆-methyladenosine

Chemical Property:

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Technology Process of N₆-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N₆-methyladenosine

There total 1 articles about N₆-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N₆-methyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N6-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylidene-N6-methyladenosine (1184837-77-1) → N6-benzoyl-8-(chloromethyl)-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-N6-methyladenosine (1184837-80-6)

Guidance literature:

N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylidene-N₆-methyladenosine; With methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 25 ℃;

With lithium chloride; In dichloromethane;

DOI:10.1002/hlca.200900075

upstream raw materials:

N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylidene-N₆-methyladenosine

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