(S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid

Base Information

• Chemical Name: (S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid
• CAS No.: 1192068-72-6
• Molecular Formula: C₂₄H₃₈N₂O₈S
• Molecular Weight: 514.64

Synonyms:(S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid

Chemical Property of (S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid

Chemical Property:

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Technology Process of (S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid

There total 1 articles about (S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid methyl ester (1192068-58-8) → (S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid (1192068-72-6)

Guidance literature:

(S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid methyl ester; With lithium hydroxide monohydrate; In tetrahydrofuran; water; at 20 ℃; for 22h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1039/b909221h

Reference yield: 99.0%

(S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid (1192068-72-6) + trifluoroacetic acid (76-05-1) → (S)-2-((S)-2-aminothiopropionylamino)-3-{2-[2-(2-benzyloxy-ethoxy)-ethoxy]-ethoxy}propionic acid trifluoroacetate

Guidance literature:

In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1039/b909221h

upstream raw materials:

(S)-3-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}-2-((S)-2-tert-butoxycarbonylaminothiopropionylamino)propionic acid methyl ester

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