C₂₁H₃₈N₄O*C₇H₈O₃S

Base Information

Chemical Name:C₂₁H₃₈N₄O*C₇H₈O₃S
CAS No.:1519003-90-7
Molecular Formula:C₇H₈O₃S*C₂₁H₃₈N₄O
Molecular Weight:534.764
Hs Code.:

C<sub>21</sub>H<sub>38</sub>N<sub>4</sub>O*C<sub>7</sub>H<sub>8</sub>O<sub>3</sub>S

Synonyms:C₂₁H₃₈N₄O*C₇H₈O₃S

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Chemical Property of C₂₁H₃₈N₄O*C₇H₈O₃S

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Technology Process of C₂₁H₃₈N₄O*C₇H₈O₃S

There total 9 articles about C₂₁H₃₈N₄O*C₇H₈O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1519003-88-3
C₂₈H₄₄N₄O

: 104-15-4
toluene-4-sulfonic acid

: 1519003-90-7
C₂₁H₃₈N₄O*C₇H₈O₃S

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; under 2585.81 Torr; Inert atmosphere;
DOI:10.1021/ml400370w

Reference yield:

: 76272-34-9
8-Benzyl-1αH,5αH-nortropan-3-one Oxime

: 1519003-90-7
C₂₁H₃₈N₄O*C₇H₈O₃S

Guidance literature:: Multi-step reaction with 8 steps

1: sodium; propan-1-ol / toluene / 12 h / Reflux; Inert atmosphere

2: tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

3: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere

7: acetic acid / ethyl acetate / 0.5 h / 80 °C / Inert atmosphere

8: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 2585.81 Torr / Inert atmosphere

With hydrogenchloride; propan-1-ol; phosphorus pentachloride; palladium 10% on activated carbon; hydrogen; sodium; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; tert-Amyl alcohol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ml400370w

Reference yield:

: 8-benzyl-8-azabicyclo[3.2.1]octan-3-amine

: 1519003-90-7
C₂₁H₃₈N₄O*C₇H₈O₃S

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran / 72 h / 20 °C / Inert atmosphere

2: hydrogenchloride / methanol; 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4: phosphorus pentachloride / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5: dichloromethane; tert-Amyl alcohol / 0 - 20 °C / Inert atmosphere

6: acetic acid / ethyl acetate / 0.5 h / 80 °C / Inert atmosphere

7: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 2585.81 Torr / Inert atmosphere

With hydrogenchloride; phosphorus pentachloride; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; tert-Amyl alcohol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ml400370w