p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

Base Information

Chemical Name:p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile
CAS No.:890531-65-4
Molecular Formula:C₂₀H₂₅N₃O₉
Molecular Weight:451.433
Hs Code.:

Synonyms:p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

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Chemical Property of p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

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Technology Process of p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

There total 5 articles about p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 890531-64-3
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-gluco-hexodialdo-1,5-pyranoside

: 890531-65-4
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

Guidance literature:: With ammonium hydroxide; iodine; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1002/ejoc.200500755

Reference yield:

: 890531-57-4
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranoside

: 890531-65-4
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

Guidance literature:: Multi-step reaction with 2 steps

1: (ClCO)2; DMSO; Et₃N / CH₂Cl₂ / -70 - 20 °C

2: 35 mg / I₂; aq. NH₃ / tetrahydrofuran / 5 h / 20 °C

With ammonium hydroxide; oxalyl dichloride; iodine; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 1: Swern oxidation;
DOI:10.1002/ejoc.200500755

Reference yield:

: 824-78-2
4-nitrophenol sodium salt

: 890531-65-4
p-nitrophenyl 2-acetamido-2-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-β-D-glucopyranosiduronitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylformamide / 16 h / 20 °C

1.2: NaOMe / methanol

2.1: 79 percent / camphorsulfonic acid / methanol / 6 h / Heating

3.1: (ClCO)2; DMSO; Et₃N / CH₂Cl₂ / -70 - 20 °C

4.1: 35 mg / I₂; aq. NH₃ / tetrahydrofuran / 5 h / 20 °C

With ammonium hydroxide; oxalyl dichloride; camphor-10-sulfonic acid; iodine; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 3.1: Swern oxidation;
DOI:10.1002/ejoc.200500755