2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol

Base Information

• Chemical Name: 2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol
• CAS No.: 2422-83-5
• Molecular Formula: C₃₄H₄₄Cl₂O₃
• Molecular Weight: 571.628
• Mol file: 2422-83-5.mol

Synonyms:2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol

Chemical Property of 2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol

There total 1 articles about 2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-<3-<3-(Hydroxymethyl)-5-tert-butylsalicyl>-5-tert-butylsalicyl>-5-tert-butyl-2-hydroxybenzyl Alcohol (65566-87-2) → 2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol (2422-83-5)

Guidance literature:

With thionyl chloride; In benzene; for 5h; Ambient temperature;

DOI:10.1246/cl.1996.183

Reference yield: 18.0%

2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol (2422-83-5) + (S)-2-((S)-2-Amino-3-phenyl-propionylamino)-3-[(S)-2-((S)-2-amino-3-phenyl-propionylamino)-2-methoxycarbonyl-ethyldisulfanyl]-propionic acid methyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT → C94H118N4O12S2

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 18h;

DOI:10.1021/jo000738z

Reference yield: 18.0%

2-<3-(3-chloromethyl-5-tert-butylsalicyl)-5-tert-butylsalicyl>-6-chloromethyl-4-tert-butylphenol (2422-83-5) + (S)-2-((R)-2-Amino-3-phenyl-propionylamino)-3-[(S)-2-((R)-2-amino-3-phenyl-propionylamino)-2-methoxycarbonyl-ethyldisulfanyl]-propionic acid methyl ester; hydrochloride → C94H118N4O12S2

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 12h;

DOI:10.1080/00397910008087057

upstream raw materials:

3-<3-<3-(Hydroxymethyl)-5-tert-butylsalicyl>-5-tert-butylsalicyl>-5-tert-butyl-2-hydroxybenzyl Alcohol