N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

Base Information

Chemical Name:N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide
CAS No.:260360-34-7
Molecular Formula:C₆₂H₈₁N₁₃O₁₆
Molecular Weight:1264.4
Hs Code.:

N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

Synonyms:N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

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Chemical Property of N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

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Technology Process of N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

There total 5 articles about N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115196-80-0
ethyl 2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)(4-azido-3-O-benzyl-4,6-dideoxy-1-thio-α-D-mannopyranoside

: 260360-34-7
N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / N-iodosuccinimide; AgOTf; MS₄A / toluene; CH₂Cl₂ / 5 - 10 °C

2: NaOMe

3: 72 percent / N-iodosuccinimide; AgOTf; MS₄A / toluene; CH₂Cl₂ / 5 - 10 °C

4: NaOMe

With N-iodo-succinimide; sodium methylate; silver trifluoromethanesulfonate; In dichloromethane; toluene; 1: Condensation / 2: Zemplen deacetylation / 3: Substitution / 4: Zemplen deacetylation;
DOI:10.1016/S0008-6215(99)00185-8

Reference yield:

: 203861-78-3
N-(2,2-dimethoxyethyl)-6-hydroxy hexanamide

: 260360-34-7
N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / N-iodosuccinimide; AgOTf; MS₄A / toluene; CH₂Cl₂ / 5 - 10 °C

2: NaOMe

3: 72 percent / N-iodosuccinimide; AgOTf; MS₄A / toluene; CH₂Cl₂ / 5 - 10 °C

4: NaOMe

With N-iodo-succinimide; sodium methylate; silver trifluoromethanesulfonate; In dichloromethane; toluene; 1: Condensation / 2: Zemplen deacetylation / 3: Substitution / 4: Zemplen deacetylation;
DOI:10.1016/S0008-6215(99)00185-8

Reference yield:

: 260360-32-5
N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)oxy]hexanamide

: 260360-34-7
N-(2,2-dimethoxyethyl)-6-[4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1->2)-bis(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-annopyranosyl)oxy]hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / N-iodosuccinimide; AgOTf; MS₄A / toluene; CH₂Cl₂ / 5 - 10 °C

2: NaOMe

With N-iodo-succinimide; sodium methylate; silver trifluoromethanesulfonate; In dichloromethane; toluene; 1: Substitution / 2: Zemplen deacetylation;
DOI:10.1016/S0008-6215(99)00185-8