1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate

Base Information

• Chemical Name: 1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate
• CAS No.: 1260086-04-1
• Molecular Formula: C₁₃H₁₀ClF₆NO₃
• Molecular Weight: 377.671

Synonyms:1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate

Chemical Property of 1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate

Chemical Property:

Purity/Quality:

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Technology Process of 1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate

There total 1 articles about 1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

N-(3-chloro-2-hydroxypropyl)aniline (76226-32-9,15949-12-9) + trifluoroacetic anhydride (407-25-0) → 1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate (1260086-04-1)

Guidance literature:

N-(3-chloro-2-hydroxypropyl)aniline; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

trifluoroacetic anhydride; In tetrahydrofuran; at -78 - 0 ℃;

DOI:10.1055/s-0030-1257938

Reference yield:

1-chloro-3-(2,2,2-trifluoro-N-phenylacetamido)propan-2-yl 2,2,2-trifluoroacetate (1260086-04-1) → N-(3-chloro-2-hydroxypropyl)aniline (76226-32-9,15949-12-9)

Guidance literature:

With water;

DOI:10.1055/s-0030-1257938

upstream raw materials:

N-(3-chloro-2-hydroxypropyl)aniline

trifluoroacetic anhydride

Downstream raw materials:

N-(3-chloro-2-hydroxypropyl)aniline

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