4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

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Chemical Name:4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene
CAS No.:57590-54-2
Molecular Formula:C₁₆H₂₃BNP
Molecular Weight:271.15
Hs Code.:

Synonyms:4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

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Technology Process of 4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

There total 2 articles about 4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 638-21-1
phenylphosphane

: 5271-93-2
Diethylamino-di--boran

: 57590-54-2
4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In hexane; under Ar, educts and AIBN refluxed in hexane for 3 h, more AIBN added, refluxed for further 3 h; distn.; elem. anal.;
DOI:10.1016/0022-328X(83)85038-4

Reference yield:

: 57590-54-2
4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

Guidance literature:: /BRN= 970298/, Phenylphosphin;

Reference yield: 82.0%

: 57590-54-2
4-diethylamino-2,6-dimethyl-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

: 87367-38-2
2,6-dimethyl-4-methoxy-1-phenyl-1-λ3-phospha-4-bora-2,5-cyclohexadiene

Guidance literature:: With methanol; In hexane; byproducts: diethylamine; under Ar, anhyd. MeOH and hexane dropped with stirring at 0°C over 70 min to soln. of educt in hexane, heated under reflux for 1 h; evapd. at 10 Torr, residue distd.; elem. anal.;
DOI:10.1016/0022-328X(83)85038-4