C₄₄H₅₃N₆O₇PS

Base Information

• Chemical Name: C₄₄H₅₃N₆O₇PS
• CAS No.: 1377975-50-2
• Molecular Formula: C₄₄H₅₃N₆O₇PS
• Molecular Weight: 840.981
• Mol file: 1377975-50-2.mol

Synonyms:C₄₄H₅₃N₆O₇PS

Chemical Property of C₄₄H₅₃N₆O₇PS

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₄H₅₃N₆O₇PS

There total 3 articles about C₄₄H₅₃N₆O₇PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C35H36N4O6S (1377975-47-7) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → C44H53N6O7PS (1377975-50-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/ejoc.201200231

Reference yield:

2,1,3-benzothiadiazole-4,7-dicarboxylic acid (5170-41-2) → C44H53N6O7PS (1377975-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201200231

Reference yield:

benzo[c][1,2,5]thiadiazole-4,7-dicarbonitrile (20138-79-8) → C44H53N6O7PS (1377975-50-2)

Guidance literature:

Multi-step reaction with 3 steps

1: water; sodium hydroxide / 2 h / 100 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

With water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201200231

upstream raw materials:

benzo[c][1,2,5]thiadiazole-4,7-dicarbonitrile

C₃₅H₃₆N₄O₆S

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

2,1,3-benzothiadiazole-4,7-dicarboxylic acid