1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

Base Information

Chemical Name:1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal
CAS No.:112807-61-1
Molecular Formula:C₂₀H₁₃NO₃
Molecular Weight:315.328
Hs Code.:

Synonyms:1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

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Chemical Property of 1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

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Technology Process of 1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

There total 3 articles about 1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82577-12-6
2-Methyl-4-oxo-1-phenyl-1,4-dihydro-indeno[1,2-b]pyrrole-3-carboxylic acid ethyl ester

: 112807-61-1
1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

Guidance literature:: Multi-step reaction with 3 steps

1: 23.2 percent / pyridine chlorohydrate / 1 h / 200 - 220 °C

2: 62 percent / AlCl₃ / benzene / 1.) 20 deg C, 20 min, 2.) 20 deg C, 1.5 h; 50-55 deg C, 0.5 h

3: 43.7 percent / SeO₂ / dioxane; H₂O / 3.5 h / Heating

With aluminium trichloride; selenium(IV) oxide; pyridine hydrochloride; In 1,4-dioxane; water; benzene;
DOI:10.1007/BF00758135

Reference yield:

: 112807-66-6
1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrole

: 112807-61-1
1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / AlCl₃ / benzene / 1.) 20 deg C, 20 min, 2.) 20 deg C, 1.5 h; 50-55 deg C, 0.5 h

2: 43.7 percent / SeO₂ / dioxane; H₂O / 3.5 h / Heating

With aluminium trichloride; selenium(IV) oxide; In 1,4-dioxane; water; benzene;
DOI:10.1007/BF00758135

Reference yield:

: 82577-26-2
1-Phenyl-2-methyl-3-carboxy-4-oxoindeno<1,2-b>pyrrole

: 112807-61-1
1-Phenyl-2-methyl-4-oxoindeno<1,2-b>pyrrolyl-3-glyoxal

Guidance literature:: Multi-step reaction with 3 steps

1: 25.6 percent / Cu, quinoline / 0.08 h / 230 °C

2: 62 percent / AlCl₃ / benzene / 1.) 20 deg C, 20 min, 2.) 20 deg C, 1.5 h; 50-55 deg C, 0.5 h

3: 43.7 percent / SeO₂ / dioxane; H₂O / 3.5 h / Heating

With quinoline; aluminium trichloride; selenium(IV) oxide; copper; In 1,4-dioxane; water; benzene;
DOI:10.1007/BF00758135