methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

Base Information

Chemical Name:methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate
CAS No.:82159-63-5
Molecular Formula:C₃₁H₃₁NO₈
Molecular Weight:545.589
Hs Code.:

Synonyms:methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

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Chemical Property of methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

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Technology Process of methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

There total 3 articles about methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 82159-62-4
methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-glycero-D-galacto-non-2-en-onate

: 82159-63-5
methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

Guidance literature:: With manganese(IV) oxide; In chloroform; at 25 ℃; for 4h;
DOI:10.1016/S0008-6215(00)80690-4

Reference yield:

: 25875-99-4,79026-38-3
methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-D-glycero-D-galacto-non-2-enonate

: 82159-63-5
methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / 48 h / 25 °C

2: 80 percent / manganese dioxide / CHCl₃ / 4 h / 25 °C

With pyridine; manganese(IV) oxide; In chloroform;
DOI:10.1016/S0008-6215(00)80690-4

Reference yield:

: 76-83-5
trityl chloride

: 82159-63-5
methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-9-O-trityl-D-manno-non-2-en-4-ulosonate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / 48 h / 25 °C

2: 80 percent / manganese dioxide / CHCl₃ / 4 h / 25 °C

With pyridine; manganese(IV) oxide; In chloroform;
DOI:10.1016/S0008-6215(00)80690-4