methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Base Information

Chemical Name:methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside
CAS No.:115196-98-0
Molecular Formula:C₄₀H₅₅N₃O₁₀
Molecular Weight:737.891
Hs Code.:

methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Synonyms:methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

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Chemical Property of methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

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Technology Process of methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

There total 8 articles about methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115196-86-6
methyl O-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

: 115196-98-0
methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: With hydrogen sulfide; In pyridine; water; at 40 ℃; for 12h;

Reference yield:

: 115234-11-2
ethyl 2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-1-thio-α-D-mannopyranoside

: 115196-98-0
methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / 0.1 M sodium methoxide / methanol / 8 h

2: 75 percent / 4 Angstroem molecular sieves, silver triflate / CH₂Cl₂ / 2 h / -70 °C

3: 80 percent / 4 Angstroem molecular sieves, methyl triflate / CH₂Cl₂ / 48 h

4: 99 percent / 0.1M sodium methoxide / methanol / 5 h / 20 °C

5: H₂S / pyridine; H₂O / 12 h / 40 °C

With 4 A molecular sieve; hydrogen sulfide; sodium methylate; silver trifluoromethanesulfonate; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water;

Reference yield:

: 117107-69-4
1,2-Di-O-acetyl-4-azido-4,6-dideoxy-3-O-benzyl-α-D-mannopyranoside

: 115196-98-0
methyl O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-O-(4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1->2)-4-amino-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 88 percent / boron trifluoride etherate, 4 Angstroem molecular sieves / CH₂Cl₂ / 2 h / Ambient temperature

2: 95 percent / 0.1 M sodium methoxide / methanol / 8 h

3: 75 percent / 4 Angstroem molecular sieves, silver triflate / CH₂Cl₂ / 2 h / -70 °C

4: 80 percent / 4 Angstroem molecular sieves, methyl triflate / CH₂Cl₂ / 48 h

5: 99 percent / 0.1M sodium methoxide / methanol / 5 h / 20 °C

6: H₂S / pyridine; H₂O / 12 h / 40 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen sulfide; sodium methylate; silver trifluoromethanesulfonate; methyl trifluoromethanesulfonate; In pyridine; methanol; dichloromethane; water;