N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

Base Information

Chemical Name:N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline
CAS No.:1365120-05-3
Molecular Formula:C₃₈H₃₇N₃O
Molecular Weight:551.731
Hs Code.:

Synonyms:N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

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Chemical Property of N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

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Technology Process of N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

There total 4 articles about N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-12-7
1,3,3-Trimethyl-2-methyleneindoline

: C₂₆H₂₄N₂O₂

: 1365120-05-3
N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

Guidance literature:: In ethanol; at 100 ℃; for 3h;
DOI:10.1016/j.tetlet.2012.02.082

Reference yield:

: 1365119-89-6
4-(4-(diethylamino)phenyl)-3-phenylnaphthalene-1,2-dione

: 1365120-05-3
N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride / ethanol / 18 h / 20 °C

2: ethanol / 3 h / 100 °C

With hydroxylamine hydrochloride; In ethanol;
DOI:10.1016/j.tetlet.2012.02.082

Reference yield:

: 123135-53-5
4--1,2-naphthoquinone

: 1365120-05-3
N,N-diethyl-4-(1,3,3-trimethyl-5'-phenylspiro[indoline-2,3'-naphtho[2,1-b][1,4]oxazin]-6'-yl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium peroxydisulfate; silver nitrate / water; 1,2-dichloro-ethane / 5 h

2: hydroxylamine hydrochloride / ethanol / 18 h / 20 °C

3: ethanol / 3 h / 100 °C

With ammonium peroxydisulfate; hydroxylamine hydrochloride; silver nitrate; In ethanol; water; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.02.082