(1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

Base Information

Chemical Name:(1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride
CAS No.:143564-22-1
Molecular Formula:C₇H₁₅NO₄*ClH
Molecular Weight:213.661
Hs Code.:

Synonyms:(1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

Chemical Property:

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Technology Process of (1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

There total 12 articles about (1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143465-64-9
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

: 143564-22-1
(1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium dihydroxide; In methanol;
DOI:10.1016/0040-4039(92)80009-9

Reference yield:

: 106265-19-4
(1S,2S,3R,4R)-3,4-di-O-benzyl-2-benzylamino-1,2-N,O-carbonyl-5-methoxymethylene-1,3,4-cyclohexanetriol

: 143564-22-1
(1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Hg(OAc)2, 2.) NaBH₄ / 1.) MeCN, H₂O, 0 deg C

2: 62 percent / NaOH / ethanol / Heating

3: H₂, HCl / 20percent Pd(OH)2 / methanol

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate; hydrogen; palladium dihydroxide; In methanol; ethanol;
DOI:10.1016/0040-4039(92)80009-9

Reference yield:

: 106265-22-9,106295-31-2,143465-48-9,143465-62-7
(3aS,4R,5R,7aS)-3-Benzyl-4,5-bis-benzyloxy-6-hydroxymethyl-hexahydro-benzooxazol-2-one

: 143564-22-1
(1S,2S,3R,4R,5R)-2-amino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NaOH / ethanol / Heating

2: H₂, HCl / 20percent Pd(OH)2 / methanol

With hydrogenchloride; sodium hydroxide; hydrogen; palladium dihydroxide; In methanol; ethanol;
DOI:10.1016/0040-4039(92)80009-9