C₂HF₃O₂*C₂₉H₃₂N₄O₂

Base Information

Chemical Name:C₂HF₃O₂*C₂₉H₃₂N₄O₂
CAS No.:1352035-50-7
Molecular Formula:C₂HF₃O₂*C₂₉H₃₂N₄O₂
Molecular Weight:582.623
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>29</sub>H<sub>32</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₂HF₃O₂*C₂₉H₃₂N₄O₂

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Chemical Property of C₂HF₃O₂*C₂₉H₃₂N₄O₂

Chemical Property:

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Technology Process of C₂HF₃O₂*C₂₉H₃₂N₄O₂

There total 9 articles about C₂HF₃O₂*C₂₉H₃₂N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352036-25-9
C₃₉H₄₈N₄O₆

: 1352035-50-7
C₂HF₃O₂*C₂₉H₃₂N₄O₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.10.009

Reference yield:

: 1352036-25-9
C₃₉H₄₈N₄O₆

: 76-05-1
trifluoroacetic acid

: 1352035-50-7
C₂HF₃O₂*C₂₉H₃₂N₄O₂

Guidance literature:: In dichloromethane; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 16535-98-1
3-hydroxy-6,7-dimethoxy-1-methylisoquinoline

: 1352035-50-7
C₂HF₃O₂*C₂₉H₃₂N₄O₂

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / dichloromethane / 0.5 h / -78 °C

2: caesium carbonate / palladium diacetate; XPhos / acetonitrile; water / 5 h / 100 °C

3: triethylamine / dichloromethane / 0.5 h / -78 °C

4: potassium carbonate / palladium diacetate; XPhos / acetonitrile; water / 2 h / 95 °C

5: selenium(IV) oxide / 1,4-dioxane / 3 h / 102 °C

6: ethanol; sodium tetrahydroborate / 1 h / 20 °C

7: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 3.25 h / 0 - 20 °C

8: dichloromethane / 2 h / 20 °C / Cooling with ice

With selenium(IV) oxide; sodium tetrahydroborate; ethanol; di-isopropyl azodicarboxylate; potassium carbonate; caesium carbonate; triethylamine; triphenylphosphine; palladium diacetate; XPhos; In 1,4-dioxane; dichloromethane; water; toluene; acetonitrile;