(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

Base Information

Chemical Name:(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile
CAS No.:102342-02-9
Molecular Formula:C₁₉H₂₀ClNO₂
Molecular Weight:329.826
Hs Code.:

Synonyms:(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

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Chemical Property of (chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

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Technology Process of (chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

There total 3 articles about (chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 102336-82-3,102336-83-4,114905-53-2,114976-47-5
(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 oxo-4 pentane carbonitrile

: 102342-02-9
(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In methanol; water; at 0 - 5 ℃; for 2h;
DOI:10.1016/0223-5234(87)90266-2

Reference yield:

: 19924-43-7
3-methoxyphenylacetonitrile

: 102342-02-9
(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium methylate / methanol / 4 h / 60 °C

2: 99 percent / sodium borohydride, sodium hydroxide / methanol; H₂O / 2 h / 0 - 5 °C

With sodium hydroxide; sodium tetrahydroborate; sodium methylate; In methanol; water;
DOI:10.1016/0223-5234(87)90266-2

Reference yield:

: 30626-03-0
(3E)-4-(4-chlorophenyl)-3-buten-2-one

: 102342-02-9
(chloro-4 phenyl)-2 (methoxy-3 phenyl)-1 hydroxy-4 pentane carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium methylate / methanol / 4 h / 60 °C

2: 99 percent / sodium borohydride, sodium hydroxide / methanol; H₂O / 2 h / 0 - 5 °C

With sodium hydroxide; sodium tetrahydroborate; sodium methylate; In methanol; water;
DOI:10.1016/0223-5234(87)90266-2