(2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Base Information

Chemical Name:(2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate
CAS No.:137344-97-9
Molecular Formula:C₂₃H₂₃F₃N₂O₈S
Molecular Weight:544.505
Hs Code.:

Synonyms:(2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Suppliers and Price of (2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

There total 3 articles about (2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 137344-96-8
2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allonhydroximo-1,5-lactone

: 137344-97-9
(2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; for 0.333333h;
DOI:10.1002/hlca.19910740625

Reference yield:

: 29873-94-7,137432-77-0,137432-78-1
2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranose

: 137344-97-9
(2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / NaOMe, NH₂OH*HCl / methanol / 4 h / 50 °C

2: 95 percent / NaIO₄, NaOAc / H₂O; ethanol / 18 h / 50 °C

3: 81 percent / NEt₃ / CH₂Cl₂ / 0.33 h

With sodium periodate; hydroxylamine hydrochloride; sodium methylate; sodium acetate; triethylamine; In methanol; ethanol; dichloromethane; water;
DOI:10.1002/hlca.19910740625

Reference yield:

: 137344-94-6,137344-95-7
2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allose oxime

: 137344-97-9
(2-Acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-D-allopyranosylidene)amino trifluormethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaIO₄, NaOAc / H₂O; ethanol / 18 h / 50 °C

2: 81 percent / NEt₃ / CH₂Cl₂ / 0.33 h

With sodium periodate; sodium acetate; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1002/hlca.19910740625