6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Base Information

Chemical Name:6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione
CAS No.:1353871-81-4
Molecular Formula:C₁₉H₁₇N₃O₅
Molecular Weight:367.361
Hs Code.:

Synonyms:6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Suppliers and Price of 6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

There total 4 articles about 6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353873-55-8
2-methyl-3,5-dioxo-4-phenyl-2,3,4,5-tetrahydro-1,2,4-triazine-6-carbonyl chloride

: 74896-14-3
1,3-bicyclo[3.2.1]octanedione

: 1353871-81-4
6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Guidance literature:: 2-methyl-3,5-dioxo-4-phenyl-2,3,4,5-tetrahydro-1,2,4-triazine-6-carbonyl chloride; 1,3-bicyclo[3.2.1]octanedione; With triethylamine; In dichloromethane; for 0.5h; Cooling with ice;

With triethylamine; 2-hydroxy-2-methylpropanenitrile; In acetonitrile; for 0.5h; Reflux;

Reference yield:

: 19102-24-0
2-methyl-4-phenyl semicarbazide

: 1353871-81-4
6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 2 h / 20 °C / Reflux

1.2: 2 h / 20 °C

2.1: hydrogenchloride; acetic acid / water / 24 h / 20 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 0.5 h / Cooling with ice

4.2: 0.5 h / Reflux

With hydrogenchloride; oxalyl dichloride; toluene-4-sulfonic acid; acetic acid; triethylamine; N,N-dimethyl-formamide; In dichloromethane; water; toluene;

Reference yield:

: 1353871-90-5
2-methyl-3,5-dioxo-4-phenyl-2,3,4,5-tetrahydro-1,2,4-triazine-6-carboxylic acid, ethyl ester

: 1353871-81-4
6-(2-hydroxy-4-oxobicyclo[3.2.1]octa-2-enylcarbonyl)-2-methyl-4-phenyl-1,2,4-triazine-3,5(2H,4H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; acetic acid / water / 24 h / 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

3.1: triethylamine / dichloromethane / 0.5 h / Cooling with ice

3.2: 0.5 h / Reflux

With hydrogenchloride; oxalyl dichloride; acetic acid; triethylamine; N,N-dimethyl-formamide; In dichloromethane; water;