Ru(C₆H₅N₂C₅H₄N)2(NO₂)2

Base Information

Chemical Name:Ru(C₆H₅N₂C₅H₄N)2(NO₂)2
CAS No.:80697-51-4
Molecular Formula:C₂₂H₁₈N₈O₄Ru
Molecular Weight:559.506
Hs Code.:

Ru(C<sub>6</sub>H<sub>5</sub>N<sub>2</sub>C<sub>5</sub>H<sub>4</sub>N)2(NO<sub>2</sub>)2

Synonyms:Ru(C₆H₅N₂C₅H₄N)2(NO₂)2

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Chemical Property of Ru(C₆H₅N₂C₅H₄N)2(NO₂)2

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Technology Process of Ru(C₆H₅N₂C₅H₄N)2(NO₂)2

There total 1 articles about Ru(C₆H₅N₂C₅H₄N)2(NO₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 73952-48-4,84027-71-4,73926-31-5,288614-83-5,131724-86-2,74006-30-7
Ru(2-(phenylazo)pyridine)2Cl₂

: 80697-51-4
Ru(C₆H₅N₂C₅H₄N)2(NO₂)2

Guidance literature:: With sodium nitrite; In ethanol; Ru complex and NaNO2 refluxing in abs. EtOH for 1.5 h, cooling to room temp. for 1 d, dark purple crystals filtering off, washing with water, EtOH and Et2O, drying in vacuo over P4O10 at room temp.; purified by recrystn. from CHCl3; identified by elem. anal., UV and IR spectra;

Reference yield: 76.0%

: 80697-51-4
Ru(C₆H₅N₂C₅H₄N)2(NO₂)2

: 123-54-6,81235-32-7
acetylacetone

: 80697-65-0
Ru(C₆H₅N₂C₅H₄N)2((CH₃CO)2CH)⁽¹⁺⁾*ClO₄^(1-)=Ru(C₆H₅N₂C₅H₄N)2((CH₃CO)2CH)ClO₄

Guidance literature:: With ammonia; In perchloric acid; Ru complex refluxing in 1 M HClO4 for 1 h, filtering hot, aq. NH3 and ligand adding, heating on a steam bath for 3 h, aq. NaClO4 adding, cooling to room temp. overnight, solid filtering off, washing with water, drying in vacuo over P4O10 at room temp.; identified by elem. anal., UV and IR spectra;