C₂₈H₂₂N₆O₂

Base Information

• Chemical Name: C₂₈H₂₂N₆O₂
• CAS No.: 1215208-28-8
• Molecular Formula: C₂₈H₂₂N₆O₂
• Molecular Weight: 474.522
• Mol file: 1215208-28-8.mol

Synonyms:C₂₈H₂₂N₆O₂

Chemical Property of C₂₈H₂₂N₆O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₂N₆O₂

There total 4 articles about C₂₈H₂₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

furfural (98-01-1) + 2,4-bis-(phenylamino)-6-(4'-acetylphenylamino)-s-triazine (84688-83-5) → C28H22N6O2 (1215208-28-8)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1016/j.ejmech.2009.10.037

Reference yield:

2-phenylamino-4,6-dichloro-s-triazine (2272-40-4) → C28H22N6O2 (1215208-28-8)

Guidance literature:

Multi-step reaction with 3 steps

1: acetone / 20 °C

2: acetone / Reflux

3: potassium hydroxide / N,N-dimethyl-formamide

With potassium hydroxide; In N,N-dimethyl-formamide; acetone;

Reference yield:

aniline (62-53-3) → C28H22N6O2 (1215208-28-8)

Guidance literature:

Multi-step reaction with 4 steps

1: acetone / 0 - 5 °C

2: acetone / 20 °C

3: acetone / Reflux

4: potassium hydroxide / N,N-dimethyl-formamide

With potassium hydroxide; In N,N-dimethyl-formamide; acetone;

upstream raw materials:

furfural

2,4-bis-(phenylamino)-6-(4'-acetylphenylamino)-s-triazine

2-phenylamino-4,6-dichloro-s-triazine

6-chloro-N,N'-diphenyl-1,3,5-triazine-2,4-diamine

Downstream raw materials:

C₂₉H₂₃N₉O

C₃₀H₂₆N₈O₂

C₃₁H₂₃N₉O

2,4-bis(phenylamino)-6-[4'-{5''-(2-furanyl)-2''-isoxazol-3''-yl}phenylamino]-s-triazine

Refernces

• 1、 Solankee, Anjani. "Synthesis and characterization of s-triazine based 1,5-benzothiazepines and isoxazoles". scheme or table. p. 993 - 997. Retrieved 2011/04/26.