(N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

Base Information

Chemical Name:(N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)
CAS No.:688365-33-5
Molecular Formula:C₄₁H₄₅N₃O₉
Molecular Weight:723.823
Hs Code.:

Synonyms:(N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

Suppliers and Price of (N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

Chemical Property:

Purity/Quality:

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Technology Process of (N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

There total 6 articles about (N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 688365-30-2
(N-t-butoxycarbonyl-O-benzyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

: 688365-33-5
(N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / H₂ / Pd/C / methanol; ethyl acetate / 18 h / 20 °C

2: 83 percent / pyridine / 18 h / 20 °C

3: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

4: 300 mg / water-soluble carbodiimide hydrochloride; 1-hydroxybenzotriazole; triethylamine / CH₂Cl₂ / 18 h / 20 °C

With pyridine; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1271/bbb.69.1733

Reference yield:

: C₁₈H₂₆N₂O₅

: 688365-33-5
(N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / H₂ / Pd/C / methanol; ethyl acetate / 18 h / 20 °C

2: 83 percent / pyridine / 18 h / 20 °C

3: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

4: 300 mg / water-soluble carbodiimide hydrochloride; 1-hydroxybenzotriazole; triethylamine / CH₂Cl₂ / 18 h / 20 °C

With pyridine; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1271/bbb.69.1733

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 688365-33-5
(N-(1-naphthyl)acetyl-O-acetyl-L-tyrosyl)-L-valyl-(di-O-acetyl-L-tyrosinol)

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / H₂ / Pd/C / methanol; ethyl acetate / 18 h / 20 °C

2: 83 percent / pyridine / 18 h / 20 °C

3: trifluoroacetic acid / CH₂Cl₂ / 1 h / 20 °C

4: 300 mg / water-soluble carbodiimide hydrochloride; 1-hydroxybenzotriazole; triethylamine / CH₂Cl₂ / 18 h / 20 °C

With pyridine; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1271/bbb.69.1733