Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate

Base Information

• Chemical Name: Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate
• CAS No.: 1008531-03-0
• Molecular Formula: C₁₈H₂₁NO₆S
• Molecular Weight: 379.434

Synonyms:Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate

Chemical Property of Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate

There total 3 articles about Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N-[4-(4-methylphenoxy)phenyl]methane sulfonamide (1017800-01-9) + methyl (2S)-glycidate (4538-50-5,85485-00-3,111058-32-3,118712-39-3) → Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate (1008531-03-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 0.666667h; microwave irradiation;

DOI:10.1016/j.tetlet.2007.11.184

Reference yield:

N-[4-(4-trifluoromethylphenoxy)phenyl]methanesulfonamide (1008530-98-0) + methyl (2S)-glycidate (4538-50-5,85485-00-3,111058-32-3,118712-39-3) → Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate (1008531-03-0)

Guidance literature:

With potassium carbonate; Heating;

DOI:10.1016/j.bmcl.2007.11.129

Reference yield:

→ Methyl (2S)-2-hydroxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate (1008531-03-0)

Guidance literature:

upstream raw materials:

N-[4-(4-methylphenoxy)phenyl]methane sulfonamide

methyl (2S)-glycidate

N-[4-(4-trifluoromethylphenoxy)phenyl]methanesulfonamide

Downstream raw materials:

Methyl (2S)-2-methoxy-3-{N-[4-(4-methylphenoxy)phenyl]-N-methanesulfonylamino}propionate

C₁₉H₂₀F₃NO₈S₂

C₁₇H₁₉NO₆S

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