2-amino-9-(4-hydroxybuta-1,2-dien-1-yl)-3,9-dihydro-6H-purin-6-one

Base Information

Chemical Name:2-amino-9-(4-hydroxybuta-1,2-dien-1-yl)-3,9-dihydro-6H-purin-6-one
CAS No.:117011-51-5
Molecular Formula:C₉H₉N₅O₂
Molecular Weight:219.203
Hs Code.:

Synonyms:6H-Purin-6-one,2-amino-1,9-dihydro-9-(4-hydroxy-1,2-butadienyl)- (9CI); 6H-Purin-6-one, 2-amino-1,9-dihydro-9-(4-hydroxy-1,2-butadienyl)-,(?à)-; Guanallene

Suppliers and Price of 2-amino-9-(4-hydroxybuta-1,2-dien-1-yl)-3,9-dihydro-6H-purin-6-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-9-(4-hydroxybuta-1,2-dien-1-yl)-3,9-dihydro-6H-purin-6-one

Chemical Property:

Vapor Pressure:4.98E-16mmHg at 25°C
Boiling Point:615.9°C at 760 mmHg
Flash Point:326.3°C
Density:1.6g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-amino-9-(4-hydroxybuta-1,2-dien-1-yl)-3,9-dihydro-6H-purin-6-one

There total 5 articles about 2-amino-9-(4-hydroxybuta-1,2-dien-1-yl)-3,9-dihydro-6H-purin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118674-17-2
(+/-)-N²-<(Dimethylamino)methylene>-N⁹-(4-hydroxy-1,2-butadien-1-yl)guanine

: 117011-51-5
(+/-)-Guanallene

Guidance literature:: With ammonia; In methanol; for 16h; Ambient temperature;
DOI:10.1021/ja00197a063

Reference yield:

: 121653-93-8
2-Amino-6-chloro-N⁹-(4-chloro-2-butyn-1-yl)purine

: 117011-51-5
(+/-)-Guanallene

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / aq. HCl / 18 h / Heating

2: 60 percent / dimethylformamide / Ambient temperature; overnight

3: t-BuOK / dimethylformamide / 5 h / 80 °C

4: NH₃ / methanol / 16 h / Ambient temperature

With hydrogenchloride; potassium tert-butylate; ammonia; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00197a063

Reference yield:

: 99776-30-4
N⁹-(4-Hydroxy-2-butyn-1-yl)guanine

: 117011-51-5
(+/-)-Guanallene

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / dimethylformamide / Ambient temperature; overnight

2: t-BuOK / dimethylformamide / 5 h / 80 °C

3: NH₃ / methanol / 16 h / Ambient temperature

With potassium tert-butylate; ammonia; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00197a063