{bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate

Base Information

Chemical Name:{bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate
CAS No.:137919-01-8
Molecular Formula:C₂₁H₂₅N₂Zr*C₂₄H₂₀B
Molecular Weight:715.901
Hs Code.:

Synonyms:{bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate

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Chemical Property of {bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate

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Technology Process of {bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate

There total 1 articles about {bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 137365-76-5
bis(η5-cyclopentadienyl){η2-α-(dimethylamino)benzyl}methylzirconium(IV)

: 64167-39-1
tri(n-butyl)ammonium tetraphenylborate

: 137919-01-8
{bis(η5-cyclopentadienyl)(α-(dimethylamino)benzyl)(acetonitrile)zirconium(IV)} tetraphenylborate

Guidance literature:: With acetonitrile; In tetrahydrofuran; under N2 or Ar or under vac.; addn. of borate in THF to soln. of Zr-complex in THF (over 30 min), mixt. cooled (0°C), stirred (12 h), concn., addn. of ether, pptn., decantation, evapn., washed (ether), evapn., soln. (MeCN), stirred (15 min); stripped to dryness, soln. (MeCN), addn. of ether, pptn. after 12 h, decantation, dried (flow of N2); elem. anal.;
DOI:10.1021/om00038a006