(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

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Chemical Name:(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine
CAS No.:252289-78-4
Molecular Formula:C₅₀H₈₃N₅O₁₀
Molecular Weight:914.237
Hs Code.:

(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

Synonyms:(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

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Chemical Property of (3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

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Technology Process of (3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

There total 10 articles about (3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 252289-77-3
C₅₀H₇₃N₅O₁₅

: 252289-78-4
(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 70 ℃; for 24h;
DOI:10.1021/jo991042c

Reference yield:

: 111-95-5
Bis-(2-methoxyethyl)amine

: 252289-78-4
(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 10.11 g / Et₃N / tetrahydrofuran / 4.5 h / 0 - 20 °C

2: 97 percent / MeNH₂ / methanol; H₂O / 8 h / 20 °C

3: 77 percent / K₂CO₃ / tetrahydrofuran / 24 h / 65 °C

4: 71 percent / methanol; H₂O / 24 h / 20 °C

5: 80 percent / LiAlH₄ / tetrahydrofuran / 24 h / 70 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; methylamine; In tetrahydrofuran; methanol; water; 1: Substitution / 2: Hydrolysis / 3: Etherification / 4: Substitution / 5: Reduction;
DOI:10.1021/jo991042c

Reference yield:

: 25081-39-4
methyl 3,5-dimethylbenzoate

: 252289-78-4
(3-[3-(3,5-bis-{[bis-(2-methoxy-ethyl)-amino]-methyl}-phenoxymethyl)-5-methylaminomethyl-benzyloxy]-5-{[bis-(2-methoxy-ethyl)-amino]-methyl}-benzyl)-bis-(2-methoxy-ethyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 58 percent / NBS; dibenzoyl peroxide / CCl₄ / 1 h / Heating; irradiation

2: 77 percent / K₂CO₃ / tetrahydrofuran / 24 h / 65 °C

3: 71 percent / methanol; H₂O / 24 h / 20 °C

4: 80 percent / LiAlH₄ / tetrahydrofuran / 24 h / 70 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; potassium carbonate; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; water; 1: Bromination / 2: Etherification / 3: Substitution / 4: Reduction;
DOI:10.1021/jo991042c