1,3-Dithiolane-2,4,5-trithione

Base Information

• Chemical Name: 1,3-Dithiolane-2,4,5-trithione
• CAS No.: 123399-69-9
• Molecular Formula: C₃S₅
• Molecular Weight: 196.363
• DSSTox Substance ID: DTXSID80365801
• Nikkaji Number: J943.611A
• Wikidata: Q82150767
• Mol file: 123399-69-9.mol

Synonyms:1,3-dithiolane-2,4,5-trithione;123399-69-9;1,3-Dithiol-2,4,5-trithione;1,3-dithiole-2,4,5-trithione;DTXSID80365801;AKOS001016875

Chemical Property of 1,3-Dithiolane-2,4,5-trithione

Chemical Property:

• Vapor Pressure: 0.004mmHg at 25°C
• Refractive Index: 1.983
• Boiling Point: 289.766 °C at 760 mmHg
• Flash Point: 129.046 °C
• PSA: 146.87000
• Density: 1.894 g/cm³
• LogP: 2.40610
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 0
• Exact Mass: 195.86035587
• Heavy Atom Count: 8
• Complexity: 151

Purity/Quality:

98%Min ^*data from raw suppliers

1,3-DITHIOLANE-2,4,5-TRITHIONE 95.00% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1(=S)C(=S)SC(=S)S1

Technology Process of 1,3-Dithiolane-2,4,5-trithione

There total 1 articles about 1,3-Dithiolane-2,4,5-trithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

bis(tetraetylammonium) bis(thioxo-1,3-dithiole-4,5-dithiolato)zincate(II) → 1,3-dithiol-2,4,5-trithione (85931-57-3,123399-69-9)

Guidance literature:

With iodine; In ethanol; acetone; at 50 ℃; for 2h;

DOI:10.1002/jhet.5570420515

Reference yield: 32.7%

2-(2-phenylethynyl)pyridine (13141-42-9) + 1,3-dithiol-2,4,5-trithione (85931-57-3,123399-69-9) → 5-phenyl-6-(pyridine-2-yl)-[1,3]dithiolo[4,5-b][1,4]dithiine-2-thione

Guidance literature:

In toluene; for 20h; Reflux; Inert atmosphere;