P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

Base Information

Chemical Name:P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide
CAS No.:142087-72-7
Molecular Formula:C₁₅H₁₈NOP
Molecular Weight:259.288
Hs Code.:

Synonyms:P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

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Technology Process of P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

There total 15 articles about P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1421840-48-3
(S)-4-chloro-2-[(1R)-1-{[(4-methylphenyl)sulfonyl]amino}ethyl]phenylmesityl(phenyl)phosphinate

: 142087-72-7,142185-06-6
(+)-(S)-P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

Guidance literature:: With lithium amide; ammonia; In tetrahydrofuran; at -78 - -70 ℃; for 1h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201500350

Reference yield:

: 1323156-96-2
C₂₂H₂₄NOP

: 142087-72-7
P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h; under 15001.5 Torr; Autoclave;
DOI:10.1002/ejoc.201100380

Reference yield:

: 1323156-93-9
C₁₅H₁₆BrOP

: 142087-72-7
P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / 20 °C / 15001.5 Torr / Autoclave

With palladium 10% on activated carbon; hydrogen; triethylamine; In diethyl ether; ethanol;
DOI:10.1002/ejoc.201100380