Technology Process of Silver picrate
There total 4 articles about Silver picrate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
NaOH;
In
water;
AgOH pptn., filtration, washing (water), refluxing (MeOH-water, water bath, 2 h); filtration, cooling, cryst., washing (petroleum ether), recrystn. (methanol), drying (vac.); elem. anal.;
- Guidance literature:
-
In
methanol; water;
mixed in CH3OH-H2O mixture 1:1, refluxed on a water bath for 2 h; cooled, filtered, washed with petroleum ether, recrystd. from 95% EtOH, dried in vac. over conc. H2SO4;
DOI:10.1081/SIM-120020332
- Guidance literature:
-
In
water;
picric acid was dissolved in hot water, Ag2O was added slowly and the mixt. stirred for 10 min at the same temp.;; a ppt. formed on cooling and was recrystd. twice from EtOH and once from H2O;;
DOI:10.1246/bcsj.58.525
