Technology Process of C36H70O5Si2
There total 3 articles about C36H70O5Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; diethyl methoxy borane;
In
tetrahydrofuran; methanol;
at -78 ℃;
for 3h;
optical yield given as %de;
diastereoselective reaction;
DOI:10.1016/j.tetlet.2011.07.105
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (triphenylphosphine)copper(I) hydride hexamer; phenylsilane / toluene / 24 h / 20 °C
2: methanol; pyridinium p-toluenesulfonate / dichloromethane / 0.5 h / 20 °C
3: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / 3 h / -78 °C
With
methanol; sodium tetrahydroborate; (triphenylphosphine)copper(I) hydride hexamer; diethyl methoxy borane; phenylsilane; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2011.07.105
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol; pyridinium p-toluenesulfonate / dichloromethane / 0.5 h / 20 °C
2: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / 3 h / -78 °C
With
methanol; sodium tetrahydroborate; diethyl methoxy borane; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.07.105