2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

Base Information

Chemical Name:2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal
CAS No.:287196-43-4
Molecular Formula:C₃₈H₄₉N₃O₁₀
Molecular Weight:707.821
Hs Code.:

Synonyms:2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

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Chemical Property of 2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

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Technology Process of 2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

There total 5 articles about 2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 287196-42-3
2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanol

: 287196-43-4
2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

Guidance literature:: With oxalyl dichloride; In dichloromethane; dimethyl sulfoxide; for 0.25h;
DOI:10.1039/b000229l

Reference yield:

: 36394-40-8
4-(2-cyanoethyl)-4-formylheptane-1,7-dinitrile

: 287196-43-4
2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

Guidance literature:: Multi-step reaction with 6 steps

1.1: 92 percent / NaBH₄ / methanol / 0 - 20 °C

2.1: 82 percent / 4-dimethylaminopyridine; triethylamine / CH₂Cl₂ / 48 h / Heating

3.1: 88 percent / NaOH; hydrazine; Raney nickel / aq. ethanol / 0.75 h / Heating

4.1: thionylchloride / 6 h

4.2: 58 percent / triethylamine / CH₂Cl₂ / 20 °C

5.1: 89 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h / Heating

6.1: 82 percent / oxalyl chloride / dimethylsulfoxide; CH₂Cl₂ / 0.25 h

With dmap; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; nickel; triethylamine; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1039/b000229l

Reference yield:

: 37414-73-6
4-(2-cyanoethyl)-4-cyclohexyliminomethylheptane-1,7-dinitrile

: 287196-43-4
2,2,2-tris[3-(2,3-dimethoxybenzamido)propyl]ethanal

Guidance literature:: Multi-step reaction with 7 steps

1.1: 92 percent / HCl / H₂O / 30 h / Heating

2.1: 92 percent / NaBH₄ / methanol / 0 - 20 °C

3.1: 82 percent / 4-dimethylaminopyridine; triethylamine / CH₂Cl₂ / 48 h / Heating

4.1: 88 percent / NaOH; hydrazine; Raney nickel / aq. ethanol / 0.75 h / Heating

5.1: thionylchloride / 6 h

5.2: 58 percent / triethylamine / CH₂Cl₂ / 20 °C

6.1: 89 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h / Heating

7.1: 82 percent / oxalyl chloride / dimethylsulfoxide; CH₂Cl₂ / 0.25 h

With hydrogenchloride; dmap; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; nickel; triethylamine; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1039/b000229l