2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane

Base Information

• Chemical Name: 2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane
• CAS No.: 1076223-47-6
• Molecular Formula: C₃₃H₅₆O₂Si₂
• Molecular Weight: 540.977
• Mol file: 1076223-47-6.mol

Synonyms:2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane

Chemical Property of 2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane

There total 1 articles about 2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undec-4-yne (1076223-46-5) → 2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane (1076223-47-6)

Guidance literature:

With 10% Pd/C; hydrogen; triethylamine; In ethyl acetate;

DOI:10.1021/ja8036433

Reference yield: 72.0%

2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undecane (1076223-47-6) → 6-(tert-butyldiphenylsilyloxy)undecan-2-ol (1076223-48-7)

Guidance literature:

With ceric ammonium nitrate; In methanol; at 0 ℃; for 6h;

DOI:10.1021/ja8036433

upstream raw materials:

2-(tert-butyldimethylsilyloxy)-6-(tert-butyldiphenylsilyloxy)undec-4-yne

Downstream raw materials:

6-(tert-butyldiphenylsilyloxy)undecan-2-ol