1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

Base Information

Chemical Name:1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether
CAS No.:152065-58-2
Molecular Formula:C₃₈H₆₂O₁₂
Molecular Weight:710.903
Hs Code.:

Synonyms:1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

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Chemical Property of 1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

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Technology Process of 1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

There total 1 articles about 1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 1204-76-8
1,2,4,5-tetrakis(hydroxymethyl)benzene

: 152065-58-2
1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 168h; Heating;
DOI:10.1021/jo00079a013

Reference yield: 34.0%

: 152065-58-2
1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

: 152065-62-8
1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; Ambient temperature;
DOI:10.1021/jo00079a013

Reference yield:

: 152065-58-2
1,2,4,5-tetrakis(4'-hydroxy-2'-oxa-1'-butyl)benzene tetra(2'-tetrahydropyranyl) ether

: 152065-66-2
1,2,4,5-tetrakis<4'-(tosyloxy)-2'-oxa-1'-butyl>benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / conc. HCl / CH₂Cl₂; methanol / Ambient temperature

2: 63 percent / aq. NaOH / tetrahydrofuran / 2 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00079a013