C₂₇H₃₃NO₄

Base Information

Chemical Name:C₂₇H₃₃NO₄
CAS No.:952596-42-8
Molecular Formula:C₂₇H₃₃NO₄
Molecular Weight:435.563
Hs Code.:

C<sub>27</sub>H<sub>33</sub>NO<sub>4</sub>

Synonyms:C₂₇H₃₃NO₄

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Chemical Property of C₂₇H₃₃NO₄

Chemical Property:

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Technology Process of C₂₇H₃₃NO₄

There total 8 articles about C₂₇H₃₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-43-0
2-iodophenylamine

: 952596-42-8
C₂₇H₃₃NO₄

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / CuI; triethylamine / PdCl₂ / acetonitrile / 4 h / 20 °C

2: 85 percent / H₂ / Pd/C / methanol / 48 h / 20 °C

3: 85 percent / NaHCO₃ / dioxane; H₂O / 12 h / 20 °C

4: 95 percent / imidazole / CH₂Cl₂ / 2 h / 20 °C

5: 93 percent / 4-(dimethylamino)pyridine / acetonitrile / 12 h / 20 °C

6: 98 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h

7: I₂; PPh₃; imidazole / benzene / 1 h / 20 °C

8: n-BuLi; HMPA / tetrahydrofuran / 4 h / -78 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; copper(l) iodide; n-butyllithium; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hydrogencarbonate; triethylamine; triphenylphosphine; palladium on activated charcoal; palladium dichloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/jo0708137

Reference yield:

: 125812-44-4
2-(2-(hydroxymethyl)ethynyl)aniline

: 952596-42-8
C₂₇H₃₃NO₄

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / H₂ / Pd/C / methanol / 48 h / 20 °C

2: 85 percent / NaHCO₃ / dioxane; H₂O / 12 h / 20 °C

3: 95 percent / imidazole / CH₂Cl₂ / 2 h / 20 °C

4: 93 percent / 4-(dimethylamino)pyridine / acetonitrile / 12 h / 20 °C

5: 98 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h

6: I₂; PPh₃; imidazole / benzene / 1 h / 20 °C

7: n-BuLi; HMPA / tetrahydrofuran / 4 h / -78 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; n-butyllithium; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hydrogencarbonate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/jo0708137

Reference yield:

: 949146-02-5
C₁₉H₂₈NO₄I

: 536-74-3
phenylacetylene

: 952596-42-8
C₂₇H₃₃NO₄

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; at -78 ℃; for 4h;
DOI:10.1021/jo0708137