N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine

Base Information

• Chemical Name: N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine
• CAS No.: 1620024-04-5
• Molecular Formula: C₄₄H₃₀N₄S
• Molecular Weight: 646.815

Synonyms:N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine

Chemical Property of N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine

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Technology Process of N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine

There total 1 articles about N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

[4-(7-bromobenzo[1,2,5]thiadiazol-4-ylethynyl)phenyl]-N,N-diphenylamine + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine (1620024-04-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; toluene; for 24h; Reflux;

DOI:10.1039/c4ob00629a

Reference yield: 80.0%

N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine (1620024-04-5) + ethenetetracarbonitrile (670-54-2) → 2-(4-(diphenylamino)phenyl)-3-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile (1620024-07-8)

Guidance literature:

In dichloromethane; at 40 ℃; for 8h;

DOI:10.1039/c4ob00629a

Reference yield: 65.0%

N-(4-(2-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)ethynyl)phenyl)-N-phenylbenzenamine (1620024-04-5) + 7,7',8,8'-tetracyanoquinodimethane (1518-16-7,6144-37-2) → 2-[4-(3,3-dicyano-1-{4-(diphenylamino)phenyl}-2-{7-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-4-yl}allylidene)cyclohexa-2,5-dien-1-ylidene]malononitrile (1620024-09-0)

Guidance literature:

In 1,2-dichloro-ethane; at 100 ℃; for 10h; Microwave irradiation;

DOI:10.1039/c4ob00629a

upstream raw materials:

4-(diphenylamino)phenyl boronic acid

Downstream raw materials:

2-(4-(diphenylamino)phenyl)-3-(4-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-7-yl)buta-1,3-diene-1,1,4,4-tetracarbonitrile

2-[4-(3,3-dicyano-1-{4-(diphenylamino)phenyl}-2-{7-(4-(diphenylamino)phenyl)benzo[c][1,2,5]thiadiazol-4-yl}allylidene)cyclohexa-2,5-dien-1-ylidene]malononitrile

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