C₅₆H₆₆Cl₃N₃O₂₈

Base Information

• Chemical Name: C₅₆H₆₆Cl₃N₃O₂₈
• CAS No.: 934682-10-7
• Molecular Formula: C₅₆H₆₆Cl₃N₃O₂₈
• Molecular Weight: 1335.5
• Mol file: 934682-10-7.mol

Synonyms:C₅₆H₆₆Cl₃N₃O₂₈

Chemical Property of C₅₆H₆₆Cl₃N₃O₂₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₆H₆₆Cl₃N₃O₂₈

There total 3 articles about C₅₆H₆₆Cl₃N₃O₂₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C61H76N2O27 (934682-06-1) → C56H66Cl3N3O28 (934682-10-7)

Guidance literature:

Multi-step reaction with 4 steps

1: 20 % Pd(OH)2/C; hydrogen / 1,4-dioxane / 20 °C

2: pyridine; dmap / 20 °C / Inert atmosphere

3: ammonium cerium (IV) nitrate / water; toluene; acetonitrile / 20 °C / Inert atmosphere

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C / Inert atmosphere

With pyridine; dmap; ammonium cerium (IV) nitrate; 20 % Pd(OH)2/C; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; dichloromethane; water; toluene; acetonitrile;

DOI:10.1002/chem.201003357

Reference yield:

C47H64N2O27 (934682-07-2) → C56H66Cl3N3O28 (934682-10-7)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine; dmap / 20 °C / Inert atmosphere

2: ammonium cerium (IV) nitrate / water; toluene; acetonitrile / 20 °C / Inert atmosphere

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C / Inert atmosphere

With pyridine; dmap; ammonium cerium (IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; water; toluene; acetonitrile;

DOI:10.1002/chem.201003357

Reference yield:

C61H72N2O29 (934682-08-3) → C56H66Cl3N3O28 (934682-10-7)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium cerium (IV) nitrate / water; toluene; acetonitrile / 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 20 °C / Inert atmosphere

With ammonium cerium (IV) nitrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; water; toluene; acetonitrile;

DOI:10.1002/chem.201003357

upstream raw materials:

C₆₁H₇₆N₂O₂₇

C₄₇H₆₄N₂O₂₇

C₆₁H₇₂N₂O₂₉

Downstream raw materials:

C₁₁₅H₁₅₉N₃O₃₉