5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

Base Information

Chemical Name:5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene
CAS No.:103886-83-5
Molecular Formula:C₂₆H₂₀Cl₂F₄S₂
Molecular Weight:543.476
Hs Code.:

Synonyms:5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

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Chemical Property of 5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

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Technology Process of 5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

There total 6 articles about 5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 933-00-6
p-methylbenzenesulfenyl chloride

: 5162-34-5
3,4,5,6-Tetrafluoro-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9,11-pentaene

: 103886-83-5
5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

Guidance literature:: With lithium perchlorate; In nitromethane; at 20 ℃; for 0.166667h;

Reference yield: 50.0%

: 933-00-6
p-methylbenzenesulfenyl chloride

: 103886-84-6
(1R,8S,11S,12S)-11-Chloro-3,4,5,6-tetrafluoro-12-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5,9-tetraene

: 103886-83-5
5-endo,8-exo-dichloro-6-exo,7-endo-di-p-tolylthio-2,3-tetrafluorobenzobicyclo<2.2.2>octene

Guidance literature:: With lithium perchlorate; In nitromethane; at 20 ℃; for 3h;

Reference yield:

: 933-00-6
p-methylbenzenesulfenyl chloride

: 103886-83-5
(1S,8R,9R,10R)-9,12-Dichloro-3,4,5,6-tetrafluoro-10,11-bis-p-tolylsulfanyl-tricyclo[6.2.2.0^2,7]dodeca-2⁽⁷⁾,3,5-triene

Guidance literature:: Multi-step reaction with 2 steps

1: nitromethane / 0.17 h

2: LiClO₄ / nitromethane

With lithium perchlorate; In nitromethane;