silver tetrakis(pentafluorophenyl)borate diethyl etherate

Base Information

Chemical Name:silver tetrakis(pentafluorophenyl)borate diethyl etherate
CAS No.:1216943-70-2
Molecular Formula:Ag*C₄H₁₀O*C₂₄BF₂₀
Molecular Weight:861.034
Hs Code.:

Synonyms:silver tetrakis(pentafluorophenyl)borate diethyl etherate

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Chemical Property of silver tetrakis(pentafluorophenyl)borate diethyl etherate

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Technology Process of silver tetrakis(pentafluorophenyl)borate diethyl etherate

There total 1 articles about silver tetrakis(pentafluorophenyl)borate diethyl etherate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 155543-02-5
lithium tetrakis(pentafluorophenyl)borate/ethyl ether complex

: silver nitrate

: 1216943-70-2
silver tetrakis(pentafluorophenyl)borate diethyl etherate

Guidance literature:: In diethyl ether; water; byproducts: LiNO3; (Ar); std. Schlenk technique; aq. soln. of Ag salt (acidified with few drops of concd. HNO3) was added dropwise to stirred soln. of Li compd. inEt2O at ambient temp.; shaken; ethereal layer septd.; washed (H2O); evapd. (vac.); dried in vac. at 60°C for 2 h; dissolved in CH2Cl2; filtered; solvent removed; dried in vac. at 50°C for 3 h; elem. anal.;
DOI:10.1021/om901063a

Reference yield: 88.0%

: 1216943-70-2
silver tetrakis(pentafluorophenyl)borate diethyl etherate

: bis(ferrocenyloxy)diphenylsilane

: [(η⁵-cyclopentadienyl)(η⁴-cyclopenta-2,4-dienone)iron(II)] tetrakis(pentafluorophenyl)borate

Guidance literature:: In dichloromethane; at -20 - 25 ℃; for 0.5h;
DOI:10.1016/j.jorganchem.2017.03.020

Reference yield: 83.0%

: 1216943-70-2
silver tetrakis(pentafluorophenyl)borate diethyl etherate

: 108-88-3,15644-74-3,16713-13-6
toluene

: silver tetrakis(pentafluorophenyl)borate toluene solvate

Guidance literature:: In toluene; byproducts: Et2O; (Ar); std. Schlenk technique; Ag compd. was dissolved in toluene at ambient temp.; evapd.; dried in vac. at 50°C for 5 h; dissolved in hot toluene; cooled to ambient temp. over 10 h; solvent removed; washed (pentane); dried in vac. at 50°C for 5 h; elem. anal.;
DOI:10.1021/om901063a