chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

Base Information

Chemical Name:chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane
CAS No.:1417536-91-4
Molecular Formula:C₂₇H₂₄ClF₅OSi
Molecular Weight:523.017
Hs Code.:

Synonyms:chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

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Chemical Property of chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

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Technology Process of chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

There total 6 articles about chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1417536-90-3
5-isopropyl-2-methyl-6-(pentafluorophenoxy)-7-phenyl-1H-indene

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1417536-91-4
chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

Guidance literature:: 5-isopropyl-2-methyl-6-(pentafluorophenoxy)-7-phenyl-1H-indene; With potassium hydride; In tetrahydrofuran; at -25 - 20 ℃;

dimethylsilicon dichloride; In tetrahydrofuran; at -25 ℃;

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 1417536-91-4
chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 48 h / 80 °C

2.1: Eaton′s Reagent / 2 h / 70 °C / Cooling with ice

3.1: aluminum (III) chloride / dichloromethane / 24.5 h / -20 - 20 °C

3.2: 20 °C

4.1: sodium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 12 h / Reflux

4.2: 1 h / 0 °C

5.1: potassium hydride / tetrahydrofuran / -25 - 20 °C

5.2: -25 °C

With aluminum (III) chloride; Eaton′s Reagent; palladium diacetate; potassium hydride; sodium carbonate; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 1417536-89-0
4-bromo-6-isopropyl-2-methyl-5-(pentafluorophenoxy)indan-1-one

: 1417536-91-4
chloro [6-isopropyl-2-methyl-5-(pentafluorophenoxy)-4-phenyl-1H-inden-1-yl] dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate; palladium diacetate; triphenylphosphine / water; 1,2-dimethoxyethane / 12 h / Reflux

1.2: 1 h / 0 °C

2.1: potassium hydride / tetrahydrofuran / -25 - 20 °C

2.2: -25 °C

With palladium diacetate; potassium hydride; sodium carbonate; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; water;