2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline

Base Information

• Chemical Name: 2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline
• CAS No.: 157226-31-8
• Molecular Formula: C₃₁H₂₉N₅
• Molecular Weight: 471.605

Synonyms:2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline

Chemical Property of 2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline

Chemical Property:

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Technology Process of 2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline

There total 1 articles about 2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl (128445-71-6) + malononitrile (109-77-3) → 2-amino-12-benzylidene-8-n-butyl-3-cyano-6,7,9,10,11,12-hexahydrobenzopyrido<2,3-j><1,10>phenanthroline (157226-31-8)

Guidance literature:

With piperidine; In ethanol; for 6h; Heating;

DOI:10.1016/0040-4020(94)00902-7

upstream raw materials:

2-amino-11-benzylidene-7-n-butyl-5,6,8,9,10,11-hexahydro-benzo<1,10>phenanthroline-3-carboxaldehyde*HCl

malononitrile

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