1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol

Base Information

• Chemical Name: 1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol
• CAS No.: 57659-76-4
• Molecular Formula: C₃₀H₁₉ClO₂
• Molecular Weight: 446.933
• Mol file: 57659-76-4.mol

Synonyms:1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol

Chemical Property of 1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol

There total 1 articles about 1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloroanthracene-9,10-dione (82-44-0) + phenylacetylene (536-74-3) → 1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol (57659-76-4)

Guidance literature:

Multistep reaction; (i) LiNH₂, dioxane, (ii) /BRN= 1912752/;

Reference yield: 68.0%

1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol (57659-76-4) → 1-Chloro-9,10-bis(phenylethynyl)anthracene (41105-35-5)

Guidance literature:

With tin(ll) chloride; In acetic acid;

Reference yield:

1-chloro-9,10-bis(phenylethynyl)-9,10-dihydroanthracene-9,10-diol (57659-76-4) → 1-Chlor-9,10-bis-(β-phenethyl)-anthracen (103329-06-2)

Guidance literature:

Multi-step reaction with 2 steps

1: SnCl₂*2H₂O, aq. AcOH / acetone / Ambient temperature

2: H₂ / Raney-Ni

With hydrogen; acetic acid; tin(ll) chloride; nickel; In acetone;

upstream raw materials:

1-chloroanthracene-9,10-dione

phenylacetylene

Downstream raw materials:

1-Chloro-9,10-bis(phenylethynyl)anthracene

1-Chlor-9,10-bis-(β-phenethyl)-anthracen