Technology Process of C20H33N3O5Si
There total 1 articles about C20H33N3O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
((S)-5-Amino-1-carbamoyl-pentyl)-carbamic acid benzyl ester; hydrochloride;
With
dmap; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 0.166667h;
2-(Trimethylsilyl)ethyl 4-nitrophenyl carbonate;
In
dichloromethane;
- Guidance literature:
-
With
triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; trifluoroacetic anhydride / tetrahydrofuran / 0.17 h / 0 - 20 °C
2.1: 10% palladium hydroxide on charcoal; hydrogen; hydrazine hydrate / methanol / 0.17 h / 0 - 20 °C / Reflux
3.1: triethylamine; magnesium sulfate / dichloromethane / 1.5 h / 20 °C
3.3: 0 - 20 °C
With
10% palladium hydroxide on charcoal; hydrogen; magnesium sulfate; hydrazine hydrate; triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; dichloromethane;