S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate

Base Information

• Chemical Name: S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate
• CAS No.: 3297-05-0
• Molecular Formula: C₁₀H₁₂O₃S₂
• Molecular Weight: 244.335

Synonyms:S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate

Chemical Property of S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate

Chemical Property:

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Technology Process of S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate

There total 4 articles about S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3,4-dimethoxybenzenediazonium tetrafluoroborate + ethyl 2-(((methylthio)carbonothioyl)oxy)-4-phenylbutanoate → S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate (3297-05-0)

Guidance literature:

With [bis(difluoromethyl)zinc(dmpu)₂]; copper(II) bis(trifluoromethanesulfonate); 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; In dimethyl sulfoxide; for 0.75h; Inert atmosphere;

DOI:10.1021/jacs.1c04254

Reference yield: 77.0%

[bis(difluoromethyl)zinc(dmpu)2] + 3,4-dimethoxybenzenediazonium tetrafluoroborate + O-(1-(4-methoxyphenyl)cyclopropyl) S-methyl carbonodithioate → S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate (3297-05-0) + 4,4-difluoro-1-(4-methoxyphenyl)butan-1-one

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; In dimethyl sulfoxide; at 20 ℃; for 0.75h; Inert atmosphere; Glovebox;

DOI:10.1021/jacs.1c04254

Reference yield:

3,4-dimethoxyaniline (6315-89-5) → S-(3,4-dimethoxyphenyl) S'-methyl carbonodithioate (3297-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrafluoroboric acid; sodium nitrite / water / 0.5 h / 0 °C

2: copper(II) bis(trifluoromethanesulfonate); 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine / dimethyl sulfoxide / 0.75 h / 20 °C / Inert atmosphere; Glovebox

With tetrafluoroboric acid; copper(II) bis(trifluoromethanesulfonate); 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; sodium nitrite; In water; dimethyl sulfoxide;

DOI:10.1021/jacs.1c04254

upstream raw materials:

3,4-dimethoxyaniline

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