(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Base Information

Chemical Name:(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate
CAS No.:1037543-20-6
Molecular Formula:C₃₉H₄₆N₄O₇
Molecular Weight:682.817
Hs Code.:

(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Synonyms:(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

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Chemical Property of (N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

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Technology Process of (N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

There total 3 articles about (N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1037543-19-3
N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-2-aminoacetamide

: (4-nitrophenoxycarbonyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

: 1037543-20-6
(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; triethylamine; at 20 ℃; for 24h;

Reference yield: 60.0%

: 1037543-19-3
N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-2-aminoacetamide

: (4-nitrophenoxycarbonyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

: 1037543-20-6
(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Guidance literature:: With triethylamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 24h;
DOI:10.1021/jm8001839

Reference yield:

: 112522-64-2
CI-994

: 1037543-20-6
(N-{[N-(2-{[4-(acetylamino)phenyl]carbonylamino}phenyl)-carbamoyl]methyl}carbamoyloxy)methyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 16 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 16 h / 0 - 5 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; triethylamine / 24 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;